I heard that letting the sample sit after adding the 5 drops of R-0003 reagent to test for combined chlorine it will revert back to pink. When I test for FC with the R-0871 my sample turns completely clear (after so many drops)--even the undissolved crystals of the R-0870 DPD powder. My tests are right on the mark when I test before and after I add a known quantity of bleach according to the Pool Calculator.
May I ask why you wait a minute after each drop of the R-9871 reagent? I add a drop, swirl a second or two and add my next drop and so on. Sometimes I'll add up to 6 drops in rapid succession because I know that I have at least 3ppm in the pool and then swirl. Maybe I'm doing it wrong.
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